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SULFENYL CHLORIDES, XII. BIS-TRICHLOROMETHANESULFENYLATED DITHIOCARBAMATES
Stajer, G.,Reisch, J.,Szabo, A. E.
, p. 99 - 104 (2007/10/02)
Mono- and bis-trichloromethanesulfenylated derivatives of aryl dithiocarbamates have been prepared.It has been found that the resulting trithiopercarbamates are unstable, and are converted in air by desulfuration into carbamates, particularly during chromatographic purification.The structure of the iminomethane derivatives obtained by sulfenylation has been verified by IR and 13C-NMR spectroscopy.
