72363-26-9

Basic information

• Product Name: C.I. 60752
• Synonyms: DISPERSE RED 92;c.i. 60752;4-[(1-amino-9,10-dihydro-4-hydroxy-9,10-dioxo-2-anthracenyl)oxy]-n-(3-ethoxypropyl)-benzenesulfonamide;4-[(1-amino-9,10-dihydro-4-hydroxy-9,10-dioxo-2-anthryl)oxy]-N-(3-ethoxypropyl)benzenesulphonamide;4-(1-AMINO-9,10-DIHYDRO-4-HYDROXY-9,10-DIOXO-2-ANTHRACENYL)OXY-N-(3-ETHOXYPROPYL)-BENZENESULFONAMIDE;Benzenesulfonamide, 4-(1-amino-9,10-dihydro-4-hydroxy-9,10-dioxo-2-anthracenyl)oxy-N-(3-ethoxypropyl)-;Disperse red 92 (C.I. 60752);Allilon Red S-BL
• CAS NO: 72363-26-9
• Molecular Formula: C₂₅H₂₄N₂O₇S
• Molecular Weight: 496.53
• EINECS: 276-602-4
• Mol File: 72363-26-9.mol

Chemical Properties

• Boiling Point: 713.7 °C at 760 mmHg
• Flash Point: 385.5 °C
• Appearance: /
• Density: 1.405
• Vapor Pressure: 4.77E-21mmHg at 25°C
• Refractive Index: 1.643
• PKA: 6?+-.0.20(Predicted)
• Water Solubility: 8.1mg/L at 20℃
• CAS DataBase Reference: C.I. 60752(CAS DataBase Reference)
• NIST Chemistry Reference: C.I. 60752(72363-26-9)
• EPA Substance Registry System: C.I. 60752(72363-26-9)

Safety Data

• Hazardous Substances Data: 72363-26-9(Hazardous Substances Data)

Usage

Uses

Used in Textile Industry:
C.I. 60752 is used as a dye for the coloring of acetic acid, polyamide, and polyester fibers. It provides good ironing fastness, light fastness, perspiration fastness, and washing fastness, with ISO ratings ranging from 4-5 for ironing and washing fastness, and 6-7 for light fastness. It also has moderate fading and staining resistance, with ISO ratings of 5 for fading and 4-5 for staining.

Preparation

1-Aminoanthracene-9,10-dione halogenating, hydrolysis, and N-(3-ethoxypropyl)-4-hydroxybenzenesulfonamide?condensation.

Flammability and Explosibility

Nonflammable

Standard

Ironing Fastness

Fading

Stain

ISO

4-5

InChI:InChI=1/C25H24N2O7S/c1-2-33-13-5-12-27-35(31,32)16-10-8-15(9-11-16)34-20-14-19(28)21-22(23(20)26)25(30)18-7-4-3-6-17(18)24(21)29/h3-4,6-11,14,27-28H,2,5,12-13,26H2,1H3

Upstream product

• 6291-85-6 3-ethoxypropylamine 
• 17418-58-5 C_. I_. disperse red 60 

Relevant articles and documents

Method for synthesizing disperse red 92

The invention relates to the field of fine chemical engineering, in particular to a method for synthesizing disperse red 92. The method comprises the following steps: dissolving disperse red 60 solidin an inert solvent for dissloving; adding chlorosulfonic acid and thionyl chloride into an obtained disperse red 60 solution, and carrying out thermal-insulation sulfonylation reaction; after the sulfonylation reaction is finished, adding sodium carbonate until a reaction solution is neutral; adding sodium carbonate and ethoxypropylamine for thermal insulation reaction; after the reaction is finished, distilling and recycling the solvent, and carrying out filter pressing and washing on an obtained material to obtain a disperse red 92 finished product. Compared with the prior art, the method has the advantages that the use amount of chlorosulfonic acid is greatly reduced, waste acid emission is reduced, and emission of a large amount of hydrogen chloride gas generated in the dilution process of excessive chlorosulfonic acid is reduced; an original two-step operation is changed into one-step operation, so that the production process is simplified; a filter pressing and washing process is omitted, so that the loss of materials in an intermediate operation process is reduced, and the yield of the product is increased.