730971-81-0Relevant articles and documents
Synthesis and spectral studies (FT-IR, 1H, 13C, 119Sn, and mass spectrometry) of mixed organotin(IV) compounds containing a long chain alkyl group (n-C7H15)
Sadiq-ur-Rehman,Ali, Saqib,Badshah, Amin
, p. 443 - 457 (2004)
Di- and triorganotin(IV) compounds of the type R2SnR 2′ and R3SnR′ (R = CH3, n-C 4H9, C6H5, C6H 5CH2 and R′ = n-C7H15) have been prepared by the reaction of R2SnCl2 and R 3SnCl with a stoichiometric amount of n-heptylmagnesium bromide, prepared in situ in dry diethyl ether. The products obtained were vacuum distilled. The structural assignments were made on the basis of spectral studies such as FT-IR, 1H, 13C, 119Sn NMR, and mass spectrometry which ascertain the tetrahedral environment around the tin atom.
