731857-25-3Relevant articles and documents
Syntheses of syn and anti doublebent [5]phenylene
Bong, Dennis T.-Y.,Chan, Eugene W. L.,Diercks, Rainer,Dosa, Peter I.,Haley, Michael M.,Matzger, Adam J.,Miljanic, Ognjen S.,Vollhardt, K. Peter C.,Bond, Andrew D.,Teat, Simon J.,Stanger, Amnon
, p. 2249 - 2252 (2007/10/03)
The parent and dipropyl-substituted anti (1a,b) and syn doublebent (2a,b) [5]phenylenes have been assembled by CpCo-catalyzed double cyclization of regiospecifically constructed appropriate hexaynes. 1H NMR, NICS, and an X-ray structural analys