76616-39-2Relevant academic research and scientific papers
Synthesis of Mono- and Bicyclic Diazasilaalkenes
Klingebiel, Uwe,Pohlmann, Sabine,Werner, Peter
, p. 1898 - 1903 (2007/10/02)
Lithium salts of hydrazones react with difluorosilanes to give the (fluorosilyl)hydrazones 1-7.The reaction of 1-7 with tert-butyllithium leads intramolecularily to the mono- and bicyclic diazasilaalkenes 8-14.Lithiated 12 reacts with chlorotrimethylsilane to give 15. - The mass and NMR spectra of the compounds are reported.
