79249-32-4Relevant academic research and scientific papers
Synthetic Approaches to 5,7- and 5,8-Dimethoxyquinoline. Sonochemical Dehalogenation of Substituted 2,4-Dichloroquinolines. Use of the 2D COLOC Spectrum for the NMR Assignment of 5,8-Dimethoxyquinoline
Osborne, A. G.,Warmsley, J. F.
, p. 1407 - 1412 (2007/10/02)
Sonochemical dehalogenation of 2,4-dichloroquinoline is very facile.However, with 5,7-dimethoxy-2,4-dichloroquinoline the reaction proceeds stepwise to provide the title dimethoxyquinolines which cannot be prepared via the Skraup reaction.The 13C NMR chemical shift assignments for 5,8-dimethoxyquinoline are presented.These were made by utilising the coupling connectivities from the bridgehead carbons in the 2D COLOC spectrum. - Keywords.Sonochemistry; Quinolines; 13C NMR Spectroscopy; 2D COLOC spectrum.
A Versatile New Synthesis of Quinolines and Related Fused Pyridines. Part 7. The Conversion of Acetamidothiophens into Thienopyridines
Meth-Cohn, Otto,Narine, Brahma,Tarnowski, Brian
, p. 1531 - 1536 (2007/10/02)
5-Substituted-2-acetamidothiophens are converted into 2-acetamidothiophen-3-carbaldehydes in good yield with equimolar amounts of dimethylformamide and phosphoryl chloride in hot dichloroethane.However, under similar conditions but with three mol of phosp
