79772-08-0Relevant academic research and scientific papers
Synthesis and characterization of Rh(CO)PPh3 and the X-ray structure of its toluene solvate
Louie, Brenda M.,Rettig, Steven J.,Storr, Alan,Trotter, James
, p. 503 - 508 (2007/10/02)
Details of the synthesis and physical properties of Rh(CO)PPh3 are given.Crystals of (triphenylphosphine)carbonylrhodium(I) - toluene (1:1) are triclinic, a = 10.690(2), b = 12.928(2), c = 13.998(2) Angstroem, α = 77.44(1), β = 83.50(1), γ = 72.70(1) deg, Z = 2, space group P1*.The structure was solved by conventional heavy-atom methods and was refined by full-matrix least-squares procedures to R = 0.039 and Rw = 0.048 for 5987 reflections with I ae 3?(I).The Rh(I) is in a distorted squareplanar environment with to Rh-N = 2.090(3) and 2.097(2), Rh-CO = 1.815(4), and Rh-P = 2.2700(8) Angstroem.The central six-membered RhGaN4 ring has a steep boat conformation with a Rh...Ga separation of 3.3819(4) Angstroem.
CARBOBNYLRHODIUM(I) DERIVATIVES OF 3,5-DIMETHYL- AND 3,5-BIS(TRIFLUOROMETHYL)PYRAZOLE
Banditelli, Guido,Bandini, Anna Laura,Bonati, Flavio,Minghetti, Giovanni
, p. 229 - 239 (2007/10/02)
Binuclear pyrazolato-bridged complexes such as 2, I or II, were obtained in alkaline solution from (OC)4Rh2Cl2 and 3,5-dimethylpyrazole (pz'H) or 3,5-bis(trifluoromethyl)pyrazole (pz''H), while in the absence of alkali (OC)2RhC
