80373-08-6Relevant academic research and scientific papers
Synthesis of 1,3,2-dioxathiolane-4-methylene-2-oxides: Potential allene oxide equivalents
Shipman, Michael,Thorpe, Heidi R.,Clemens, Ian R.
, p. 10845 - 10850 (1999)
Two complementary approaches to 1,3,2-dioxathiolane-4-methylene-2-oxides are described. For example, treatment of 2-hydroxy-2-methylbutan-3-one with thionyl chloride (Et3N, CH2Cl2, -78°C) yields 5.5-dimethyl-1,3,2- dioxath
