81751-07-7Relevant academic research and scientific papers
THE SYNTHESIS OF DEHYDROPERLOLINE
Prager, Rolf,Duong, Thach,Clarke, Stuart
, p. 237 - 239 (2007/10/02)
Fluorenone and 3-aza-4-oxo-3,4-dihydrofluorenone react with 3,4-dimethoxyphenyllithium to form the corresponding fluorenols, which react with hydrazoic acid to form the phenanthridine.The N-oxides photolyse smoothly to yield dehydroperloline and its analo
Synthetic Studies on 5-(3,4-Dimethoxyphenyl)-5,6-dihydrophenanthridin-6-ol an Analogue of Perloline
Clarke, Stuart I.,Prager, Rolf H.
, p. 1645 - 1653 (2007/10/02)
Two independent syntheses of the title compound (2), an analogue of perloline, are described. 9-(3,4-Dimethoxyphenyl)fluoren-9-ol reacted with hydrazoic acid in poliphosphoric acid to give 6-(3,4-dimethoxyphenyl)phenanthridine, the N-oxide of which was ph
