82056-41-5Relevant articles and documents
New Synthesis of Cyclopropanes from 1,3-Dicarbonyl Compounds Utilizing Electroreduction of 1,3-Dimethanesulfonates
Shono, Tatsuyo,Matsumura, Yoshihiro,Tsubata, Kenji,Sugihara, Yoshihiro
, p. 3090 - 3094 (2007/10/02)
Electroorganic synthesis of cyclopropanes from dimethanesulfonates of 1,3-diols is described.The process involves reduction of 1,3-dicarbonyl compounds with LiAlH followed by esterification with methanesulfonyl chloride and electroreduction.