847834-49-5Relevant articles and documents
One-pot cyclizations of dilithiated oximes and hydrazones with epibromohydrin. Efficient synthesis of 6-hydroxymethyl-5,6-dihydro-4H-1,2- oxazines and oxazolo[3,4-b]pyridazin-7-ones
Dang, Tuan Thanh,Albrecht, Uwe,Gerwien, Katrin,Siebert, Melanie,Langer, Peter
, p. 2293 - 2301 (2007/10/03)
The one-pot cyclization of dilithiated oximes with epibromohydrin provided a convenient and regioselective approach to 6-hydroxymethyl-5,6-dihydro-4H-1,2- oxazines. The reaction of the latter with phosphorus tribromide resulted in a Beckmann rearrangement