85608-99-7Relevant academic research and scientific papers
Convenient Methods for the Preparation of p-Dialkylaminophenylacetylenes
Akiyama, Shuzo,Nakatsuji, Shin'ichi,Yoshida, Keiko,Nakashima, Kenichiro,Hagiwara, Toshimitsu,et al.
, p. 361 - 362 (2007/10/02)
Two convenient methods for the preparation of p-dialkylaminophenylacetylenes are reported: a) Dehydrobromination of the brominated compounds obtained easily from the dialkylamino substituted cinnamic acids in acetic acid instead of chloroform; b) dehydrochlorination of the 2-chlorostyrene derivative obtained from the reaction of p-dimethylaminobenzaldehyde with chloromethylenetriphenylphosphorane.
