894797-92-3

Basic information

• Product Name: 4-benzyloxy-2-(2-methyl-[1,3]dioxolan-2-yl)-phenylboronic acid
• Synonyms: 4-benzyloxy-2-(2-methyl-[1,3]dioxolan-2-yl)-phenylboronic acid
• CAS NO: 894797-92-3
• Molecular Weight: 314.146
• Mol File: 894797-92-3.mol
• Article Data: 1

Chemical Properties

• CAS DataBase Reference: 4-benzyloxy-2-(2-methyl-[1,3]dioxolan-2-yl)-phenylboronic acid(CAS DataBase Reference)
• NIST Chemistry Reference: 4-benzyloxy-2-(2-methyl-[1,3]dioxolan-2-yl)-phenylboronic acid(894797-92-3)
• EPA Substance Registry System: 4-benzyloxy-2-(2-methyl-[1,3]dioxolan-2-yl)-phenylboronic acid(894797-92-3)

Safety Data

• Hazardous Substances Data: 894797-92-3(Hazardous Substances Data)

Upstream product

• 894762-72-2 4-benzyloxy-2-[1,1-(ethylenedioxy)ethyl]-bromobenzne 
• 105805-16-1 1-[2-bromo-5-(phenylmethoxy)phenyl]ethanone 
• 107-21-1 ethylene glycol 

Downstream Products

• 894797-91-2 2-acetyl-4-benzyloxyphenylboronic acid 

Relevant articles and documents

CHEMICAL PROCESSES AND INTERMEDIATES

The present invention provides a process for the formation of an enamide (III) wherein each R is independently selected from (1-6C)alkyl, benzyl and C(O)(1-6C)alkyl, or two RO groups together form a (1-4C)alkylenedioxy group, comprising the steps of reductive acylation of an oxime of formula (IX) wherein each R is independently selected from (1-6C)alkyl, benzyl and C(O)(1-6C)alkyl, or two RO groups together form a (1-4C)alkylenedioxy group, and the hydroxy group may optionally be protected by a hydroxy protecting group; and thereafter if necessary, removal of any protecting groups. Intermediates to the enamide (III) and methods for their preparation are also described.