91628-87-4Relevant academic research and scientific papers
triethoxysilane; synthesis and spectral characterization of 13C-substituted compounds
Jenneskens, Leonardus W.,Berg, Ellen M. M. van den,Heemskerk, Bram,Lugtenburg, Johan
, p. 627 - 630 (2007/10/02)
The synthesis of triethoxysilane (1a) from (1-13C)acrylonitrile (4a) is described.The latter was prepared from potassium (13C)cyanide (13C-enrichment >99percent) and 2-bromoethanol (7).The spectroscopic properties of the 13C-substituted compounds are discussed.
CONVENIENT SYNTHESIS FOR SELECTIVELY ISOTOPICALLY LABELED ACRYLONITRILES
Berg, E.M.M. van der,Richardson, E.E.,Lugtenburg, J.,Jenneskens, L.W.
, p. 1189 - 1198 (2007/10/02)
A convenient labscale synthesis of selectively, isotopically labelled acrylonitriles (1) from readily available and relatively inexpensive enriched starting materials is described.
