92339-72-5Relevant articles and documents
Preparation of α-Substituted S-Phenyl Thio Esters from Aldehydes and (Phenylthio)nitromethane
Barrett, Anthony G. M.,Graboski, Gregory, G.,Russell, Mark A.
, p. 1012 - 1015 (2007/10/02)
Acetaldehyde and isobutyraldehyde, RCHO, reacted with (phenylthio)nitromethane (KO-t-Bu, THF, t-BuOH) followed by methanesulfonyl chloride (Et3N, CH2Cl2) to give the (Z)-alkenes RCH=C(SPh)NO2.These reacted with the nucleophiles NuM = potassium phthalimid