93366-52-0Relevant academic research and scientific papers
A convenient method for the preparation of alkyl aryl sulfides from alcohols and (chloromethylene)dimethylammonium chloride
Kawano, Yoshikazu,Kaneko, Nobuya,Mukaiyama, Teruaki
, p. 1612 - 1613 (2005)
(Chloromethylene)dimethylammonium chloride (Vilsmeier reagent), prepared easily from DMF and oxalyl chloride, works as an efficient condensation reagent for the thioetherification of alcohols in one-pot under mild conditions. Various alcohols are successively converted into the corresponding sulfides with inversion of configurations in moderate to high yields. Copyright
ACTIVATION OF NITROSO GROUP WITH THIOLS. A NEW TRANSFORMATION OF PRIMARY AMINES TO ORGANIC SULFIDES OR THIOLS
Ueno, Yoshio,Tanaka, Chie,Okawara, Makoto
, p. 2675 - 2678 (2007/10/02)
Aliphatic primary amines reacted with 2-mercaptobenzothiazole in the presence of t-butylnitrite at room temperature to give condensation products, 2-(alkylthio)benzothiazole.
A CONVENIENT AND GENERAL SYNTHESIS OF ALKANE SULFINIC ACIDS
Ueno, Yoshio,Kojima, Akihiko,Okawara, Makoto
, p. 2125 - 2128 (2007/10/02)
2-(Alkylsulfonyl)benzothiazoles are reduced with sodium tetrahydroborate to give alkane sulfinic acids in good yield.
