93832-46-3Relevant academic research and scientific papers
STUDIES IN AZIDE CHEMISTRY. PART 12. ONE-POT CONVERSION OF 4-AZIDOTETRAFLUOROPYRIDINE TO 1,3,4-TRIFLUORO-7,9-DIMETHYL-11H-PYRIDOBENZODIAZEPINE
Banks, Ronald E.,Madany, Ismail M.
, p. 357 - 360 (2007/10/02)
Thermolysis of 4-azidotetrafluoropyridine in the presence of an excess of mesidine at 170 deg C yields tetrafluoro-4-(2,4,6-trimethylphenylazo)-pyridine, which undergoes intramolecular dehydrofluorination in situ to provide 1,3,4-trifluoro-7,9-dimethyl-11H-pyridobenzodiazepine.
