946-41-8Relevant academic research and scientific papers
One-pot catalyst-free synthesis of β-and γ-hydroxy sulfides using diaryliodonium salts and microwave irradiation
Vaddula, Buchi Reddy,Varma, Rajender S.,Leazer, John
supporting information, p. 6852 - 6855 (2013/02/22)
A simple and rapid one-pot protocol is described for the preparation of α- and β-hydroxy sulfides. The direct solvent-free microwave irradiation of diaryliodonium salts, potassium thiocyanate, and ethylene glycol/β-propylene glycol without any catalyst or base affords the final compounds in good yields (65-95 %) in around 10-25 min. Copyright
