96289-97-3

Basic information

• Product Name: (8R,9S,10R,13S,14S,17S)-17-Hydroxy-10,13-dimethyl-17-(phenylethynyl)-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-3H-cyclopenta[a]phenanthren-3-one
• Synonyms: (8R,9S,10R,13S,14S,17S)-17-Hydroxy-10,13-dimethyl-17-(phenylethynyl)-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-3H-cyclopenta[a]phenanthren-3-one
• CAS NO: 96289-97-3
• Molecular Weight: 388.55
• Mol File: 96289-97-3.mol
• Article Data: 3

Chemical Properties

• CAS DataBase Reference: (8R,9S,10R,13S,14S,17S)-17-Hydroxy-10,13-dimethyl-17-(phenylethynyl)-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-3H-cyclopenta[a]phenanthren-3-one(CAS DataBase Reference)
• NIST Chemistry Reference: (8R,9S,10R,13S,14S,17S)-17-Hydroxy-10,13-dimethyl-17-(phenylethynyl)-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-3H-cyclopenta[a]phenanthren-3-one(96289-97-3)
• EPA Substance Registry System: (8R,9S,10R,13S,14S,17S)-17-Hydroxy-10,13-dimethyl-17-(phenylethynyl)-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-3H-cyclopenta[a]phenanthren-3-one(96289-97-3)

Safety Data

• Hazardous Substances Data: 96289-97-3(Hazardous Substances Data)

Upstream product

• 591-50-4 iodobenzene 
• 434-03-7 levonorgestrel 
• 96373-79-4 17α-Hydroxy-3β-acetoxy-17β-phenylethinyl-5α-androstan 
• 96176-87-3 3β,17α-Dihydroxy-17β-phenylethinyl-5α-androstan 
• 97548-93-1 17α-(2-phenyl-1-ethynyl)-5α-androstane-3β,17β-diol 
• 481-29-8 Epiandrosterone 
• 4397-53-9 p-benzyloxybenzaldehyde 
• 63-05-8 Androstenedione 
• 114943-73-6 2-(4-Benzyloxyphenyl)-1,1-dibromoethylene 
• 104877-58-9 3β-Acetoxy-17β-methyl-17α-phenylaethinyl-18-nor-5α-androsten-(13) 

Downstream Products

• 143137-15-9 (1S,3aS,3bR,10aR,10bS,12aS)-10a,12a-Dimethyl-1-phenylethynyl-2,3,3a,3b,4,5,10,10a,10b,11,12,12a-dodecahydro-1H-7-oxa-8-aza-dicyclopenta[a,h]phenanthren-1-ol 
• 501-65-5 diphenyl acetylene 
• 143137-29-5 (8R,9S,10R,13S,14S,17S)-17-Hydroxy-2-[1-hydroxy-meth-(Z)-ylidene]-10,13-dimethyl-17-phenylethynyl-1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-cyclopenta[a]phenanthren-3-one 

Relevant articles and documents

Gram-Scale Preparation of Pd@PANI: A Practical Catalyst Reagent for Copper-Free and Ligand-Free Sonogashira Couplings

Palladium nanoparticles on the polyaniline (Pd@PANI) catalyst are now easily prepared on a gram scale through the oxidative polymerization of aniline in the presence of PdCl2 by using air as a clean oxidant. The material is found to be very stable and can be stored for more than one year without deactivation. Thus, it may become a commercial reagent in organic synthesis, depending on its application scopes. This article reported the first example of Pd@PANI-catalyzed Sonogashira couplings free of copper and ligands.

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