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CAS No.: | 123-33-1 |
---|---|
Name: | 3,6-Dihydroxypyridazine |
Article Data: | 44 |
Molecular Structure: | |
Formula: | C4H4N2O2 |
Molecular Weight: | 112.088 |
Synonyms: | 3(2H)-Pyridazinone,6-hydroxy- (6CI,7CI);1,2-Dihydro-3,6-pyridazinedione;3,6-Dioxopyridazine;3,6-Pyridazinediol;6-Hydroxy-3(2H)-pyridazinone;Antergon;Antyrost;MAH;MH;Sorbatran;SuperDe-Sprout;Yadi;Yake;MH (hydrazide);Maleic acid cyclic hydrazide;Maleic cyclic hydrazide;Maleic hydrazide;Malepin;Malzid;Mazide;NSC 13892;NSC 234167;NSC 48832;NSC 8823;Regulox 36;Royal Slo-Gro; |
EINECS: | 204-619-9 |
Density: | 1.321 g/cm3 |
Melting Point: | 299-301 °C (dec.)(lit.) |
Boiling Point: | 477.2 °C at 760 mmHg |
Flash Point: | 242.4 °C |
Solubility: | 6 g/L |
Appearance: | Crystalline |
Hazard Symbols: | Xn,Xi |
Risk Codes: | 36/37/38-40 |
Safety: | 26-36-45-36/37/39 |
Transport Information: | UN 3077 9/PG 3 |
PSA: | 65.72000 |
LogP: | -0.93680 |
Conditions | Yield |
---|---|
With hydrazine hydrate; sulfuric acid; lanthanum(lll) triflate In water at 30 - 120℃; for 10.5h; Temperature; Reagent/catalyst; | 97.2% |
With hydrazine hydrate In water at 100℃; for 3h; | 92% |
With hydrogenchloride; hydrazine hydrate In water Cooling with ice; Reflux; | 86% |
Conditions | Yield |
---|---|
With hydrazine hydrate In water at 95℃; for 3h; Reagent/catalyst; Time; | 90% |
With water; hydrazine |
1-oxy-2H-pyridazin-3-one
Maleic hydrazide
Conditions | Yield |
---|---|
With acetic anhydride |
N,N'-bis-(3c-carboxy-acryloyl)-hydrazine
Maleic hydrazide
Conditions | Yield |
---|---|
With water |
Conditions | Yield |
---|---|
Verb. 1 = 1 Mol; |
Conditions | Yield |
---|---|
In acetic acid for 3h; Reflux; |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol | 95% |
With ethanol; platinum at 100℃; under 2942.03 Torr; Hydrogenation; | |
With ethanol; aluminium amalgam |
Conditions | Yield |
---|---|
With 1-methyl-2-pyrrolidinone hydrosulfate In neat (no solvent) at 85℃; for 0.05h; Green chemistry; | 94% |
Maleic hydrazide
4-chlorobenzaldehyde
dimedone
11-(4-chlorophenyl)-3,3-dimethyl-11-3,4-dihydro-1H-pyridazino[1,2-a]indazole-1,6,9(2H,11H)-trione
Conditions | Yield |
---|---|
With 1-methyl-2-pyrrolidinone hydrosulfate In neat (no solvent) at 85℃; for 0.0833333h; Green chemistry; | 93% |
With toluene-4-sulfonic acid at 80℃; for 0.333333h; neat (no solvent); | 49% |
Maleic hydrazide
4-nitrobenzaldehdye
dimedone
3,3-dimethyl-11-(4-nitrophenyl)-2,3,4,11-tetrahydro-1H-pyridazino[1,2-a]indazole-1,6,9-trione
Conditions | Yield |
---|---|
With 1-methyl-2-pyrrolidinone hydrosulfate In neat (no solvent) at 85℃; for 0.05h; Green chemistry; | 93% |
With toluene-4-sulfonic acid at 80℃; for 0.416667h; neat (no solvent); | 48% |
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1. | cyt-grh-orl 5 mg | CYTOAN Cytologia. 37 (1972),345. | ||
2. | mma-sat 50 µL/plate | MUREAV Mutation Research. 66 (1979),247. | ||
3. | dns-esc 30 µmol/L | ZKKOBW Zeitschrift fuer Krebsforschung und Klinische Onkologie. 92 (1978),177. | ||
4. | sln-dmg-orl 4000 ppm | MUREAV Mutation Research. 55 (1978),15. | ||
5. | sln-dmg-par 4000 ppm | NATUAS Nature. 207 (1965),439. | ||
6. | cyt-mus-ipr 5000 ppm | CISCB7 CIS, Chromosome Information Service. 20 (1976),28. | ||
7. | orl-rat LD50:3800 mg/kg | WRPCA2 World Review of Pest Control. 9 (1970),119. |