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Cas Database |
| Name |
1-Methyl-3-pyrrolidinol |
EINECS | 236-189-3 |
| CAS No. | 13220-33-2 | Density | 1.045 g/cm3 |
| PSA | 23.47000 | LogP | -0.37930 |
| Solubility | N/A | Melting Point |
N/A |
| Formula | C5H11NO | Boiling Point | 192.2 °C at 760 mmHg |
| Molecular Weight | 101.148 | Flash Point | 70.6 °C |
| Transport Information | N/A | Appearance | Colorless or light yellow liquid |
| Safety | 26-36/37/39 | Risk Codes | 36/37/38 |
| Molecular Structure |
|
Hazard Symbols |
 Xi
|
| Synonyms |
1-Methyl-3-pyrrolidinol;N-Methyl-3-hydroxypyrrolidine;N-Methyl-3-pyrrolidinol;NSC 89279; |
Article Data | 13 |
1-Methyl-3-pyrrolidinol Synthetic route
- 19398-47-1
1,4-dibromo-2-butanol
- 74-89-5
methylamine
A
- 13220-33-2
1-methyl-3-pyrrolidinol
B
- 1404453-61-7
1,4-bis(methylamino)butan-2-ol
| Conditions | Yield |
|---|---|
| In water at 100℃; for 16h; Inert atmosphere; | A 98% B 0.9 g |
| Conditions | Yield |
|---|---|
| In water at 10 - 120℃; under 7500.75 Torr; for 10h; Temperature; Pressure; Autoclave; Sealed tube; | 64.8% |
- 13220-33-2
1-methyl-3-pyrrolidinol
| Conditions | Yield |
|---|---|
| 56% |
| Conditions | Yield |
|---|---|
| 25% |
- 14891-10-2
ethyl-3-oxo-1-pyrrolidinecarboxylate
- 13220-33-2
1-methyl-3-pyrrolidinol
| Conditions | Yield |
|---|---|
| With lithium aluminium tetrahydride |
| Conditions | Yield |
|---|---|
| With ethanol at 125 - 130℃; |
- 554-15-4
1-methyl-2,5-dihydro-pyrrole
- 13220-33-2
1-methyl-3-pyrrolidinol
| Conditions | Yield |
|---|---|
| With sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide Product distribution; var. hydroborating agents, olefin to hydroborating agent ratios, and times; other N-substituted-3-pyrrolines; |
- 13220-33-2
1-methyl-3-pyrrolidinol
| Conditions | Yield |
|---|---|
| With sodium tris(acetoxy)borohydride; acetic acid In tetrahydrofuran |
1-Methyl-3-pyrrolidinol Chemical Properties
IUPAC Name: 1-methylpyrrolidin-3-ol
Empirical Formula: C5H11NO
Molecular Weight: 101.1469g/mol
EINECS: 236-189-3
Structure of 3-Pyrrolidinol,1-methyl- (CAS NO.13220-33-2):
Index of Refraction: 1.496
Molar Refractivity: 28.31 cm3
Molar Volume: 96.7 cm3
Polarizability: 11.22×10-24cm3
Surface Tension: 39 dyne/cm
Density: 1.045 g/cm3
Flash Point: 70.6 °C
Enthalpy of Vaporization: 49.85 kJ/mol
Boiling Point: 192.2 °C at 760 mmHg
Vapour Pressure: 0.132 mmHg at 25°C
Chemical Properties: Clear colorless to pale yellow liquid
Product Categories: Heterocyclic Compounds;Heterocycles;Building Blocks;Heterocyclic Building Blocks;Pyrrolidines
Canonical SMILES: CN1CCC(C1)O
InChI: InChI=1S/C5H11NO/c1-6-3-2-5(7)4-6/h5,7H,2-4H2,1H3
InChIKey: FLVFPAIGVBQGET-UHFFFAOYSA-N
1-Methyl-3-pyrrolidinol Safety Profile
Hazard Codes: 
Xi
Risk Statements: 36/37/38
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36/37/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.
WGK Germany: 3
1-Methyl-3-pyrrolidinol Specification
3-Pyrrolidinol,1-methyl- , its cas register number is 13220-33-2. It also can be called 1-Methyl-3-pyrrolidinol ; EINECS 236-189-3 ; NSC 89279 . 3-Pyrrolidinol,1-methyl- (CAS NO.13220-33-2) is irritating to eyes, respiratory system and skin. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
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