Detail of "13220-33-2"

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CAS Number:
13220-33-2
Name:
3-Pyrrolidinol,1-methyl-
Superlist Name:
1-Methyl-3-pyrrolidinol
Molecular Structure:
Formula:
C₅H₁₁NO
Molecular Weight:
101.1469
Synonyms:
1-Methyl-3-pyrrolidinol;N-Methyl-3-hydroxypyrrolidine;N-Methyl-3-pyrrolidinol;NSC 89279;
EINECS:
236-189-3
Density:
1.045 g/cm³
Boiling Point:
192.2 °C at 760 mmHg
Flash Point:
70.6 °C
Appearance:
Colorless or light yellow liquid
Hazard Symbols:
Xi
Risk Codes:
36/37/38
Safety:
26-36/37/39 Details

High-performance liquid chromatographic determination of enantiomeric purity of 1-methyl-3-pyrrolidinol via derivatization with (R,R)-O,O-dibenzoyltartaric acid anhydride: High-performance liquid chromatographic determination of enantiomeric purity of 1-methyl-3-pyrrolidinol via derivatization with (R,R)-O,O-dibenzoyltartaric acid anhydride. Demian, Iulia; Gripshover, David F. (Anal. Res. Dep., A. H. Robins Co.Some commonly used reagents like 64339-95-3 and 13220-33-2 are used in this experiment., Richmond, VA 23220, USA). J. Chromatogr., 387, 532-5 (English) 1987. CODEN: JOCRAM. ISSN: 0021-9673. DOCUMENT TYPE: Journal CA Section: 80 (Organic Analytical Chemistry) The enantiomeric purity of 1-methyl-3-pyrrolidinol was detd. by its diastereomeric derivatization with (R,R)-O,O-dibenzoyltartaric acid anhydride followed by reversed-phase HPLC sepn. with UV detection. The column used was packed with Zorbax C8, and the mobile phase was MeOH-0.1% triethylamine soln. (pH 4.2). .

3-Methylflavone-8-carboxylic acid ester derivatives: 3-Methylflavone-8-carboxylic acid ester derivatives. (Hokuriku Pharmaceutical Co., Ltd., Japan). Jpn. Kokai Tokkyo Koho JP 59013773 A2 24 Jan 1984 Showa, 12 pp. (Japanese). (Japan). CODEN: JKXXAF. CLASS: IC: C07D311-30; C07D405-12. ICA: A61K031-35. APPLICATION: JP 82-122838 16 Jul 1982. DOCUMENT TYPE: Patent CA Section: 27 (Heterocyclic Compounds (One Hetero Atom)) Twenty-seven title derivs. I [R = Q (m = 0-2; k = 2, 3; R1 = alkyl) ,O(CH2)nNR2R3 (n = 2, 3; R2, R3 = alkyl, cycloalkyl, phenylalkyl; R2R3N may form a ring), CHR4CHR5NR2R3 (R4, R5 = H, Me)] useful for treatment of pollakiuria (no data) were prepd. Thus, refluxing 2,5 g I (R = Cl) with 0.In this article, certain chemicals are used. One of their cas registry numbers is 13220-33-2 76 g 1-methyl-3-pyrrolidinol in C6H6 for 2 h gave, after treating with 1.1 g fumaric acid, 1.17 g I fumarate (R = 1-methyl-3-pyrrolidinyloxy). .