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1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
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Name

1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene

 EINECS 1533716-785-6
CAS No. 41481-63-4 Density 1.172 g/cm3
PSA 60.98000 LogP 4.72980
Solubility N/A Melting Point 141-142 °C(Solv: ethanol (64-17-5))
Formula C18H18O4S Boiling Point 500.7 °C at 760 mmHg
Molecular Weight 330.405 Flash Point 256.6 °C
Transport Information N/A Appearance white powder
Safety Risk Codes N/A
Molecular Structure Molecular Structure of 41481-63-4 (1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene) Hazard Symbols N/A
Synonyms

4,4'-Diallyloxydiphenyl sulfone;Bis(4-hydroxyphenyl)sulfone diallyl ether;Bisphenol S diallyl ether;NSC 85530;

Article Data 10

1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene Synthetic route

80-09-1

4,4'-sulfonediphenol

107-05-1

3-chloroprop-1-ene

41481-63-4

4,4’-sulfonylbis((allyloxy)benzene)

Conditions
ConditionsYield
With potassium iodide; sodium hydroxide In methanol at 35 - 65℃; for 5h; Reagent/catalyst; Solvent;98%
Stage #1: 4,4'-sulfonediphenol With sodium hydroxide for 0.166667h;
Stage #2: 3-chloroprop-1-ene at 60 - 100℃; for 5h; Inert atmosphere; Sealed tube;		93%
With sodium hydroxide In methanol at 45℃;
With sodium hydroxide In water at 55 - 60℃; under 600.06 - 750.075 Torr; for 8h; Concentration; Temperature; Time;612 g
Stage #1: 4,4'-sulfonediphenol With sodium hydroxide In water; toluene at 80℃; for 8h;
Stage #2: 3-chloroprop-1-ene at 75℃; for 8h;
187737-37-7

propene

80-09-1

4,4'-sulfonediphenol

41481-63-4

4,4’-sulfonylbis((allyloxy)benzene)

Conditions
ConditionsYield
Stage #1: 4,4'-sulfonediphenol With chlorine; sodium hydroxide for 0.166667h;
Stage #2: propene at 60 - 100℃; for 5h; Inert atmosphere; Sealed tube;		96%
80-09-1

4,4'-sulfonediphenol

106-95-6

allyl bromide

41481-63-4

4,4’-sulfonylbis((allyloxy)benzene)

Conditions
ConditionsYield
Stage #1: 4,4'-sulfonediphenol With potassium carbonate In acetone for 1h; Inert atmosphere; Reflux;
Stage #2: allyl bromide In acetone Reflux; Inert atmosphere;		94%
With sodium hydroxide; tetramethylammonium bromide In water; toluene at 49.9 - 59.9℃; for 15h;
In methanol; water; toluene30.5 parts (91.2%)
With potassium carbonate In acetone at 80℃; Inert atmosphere;
80-09-1

4,4'-sulfonediphenol

107-05-1

3-chloroprop-1-ene

A

41481-63-4

4,4’-sulfonylbis((allyloxy)benzene)

B

4-allyloxy-4'-hydroxydiphenyl-sulfone

Conditions
ConditionsYield
With sodium hydroxide In water at 55 - 60℃; under 600.06 - 750.075 Torr; for 8h; Concentration; Temperature; Time;A n/a
B 93.5%
With sodium hydroxide In water at 55 - 60℃; under 600.06 - 750.075 Torr; for 4h; Concentration; Temperature; Time;A 73.98%
B 25.32%
41481-63-4

4,4’-sulfonylbis((allyloxy)benzene)

tetrabromobisphenol-S-bis-(2,3-dibromopropyl ether)

Conditions
ConditionsYield
With tetrabutylammomium bromide; bromine In chloroform; water at 15 - 35℃; for 2h; Solvent; Temperature;98%
41481-63-4

4,4’-sulfonylbis((allyloxy)benzene)

41481-66-7

3,3′-diallyl-4,4′-dihydroxydiphenylsulfone

Conditions
ConditionsYield
With α-alanine-N-diacetic acid at 198 - 200℃; for 7h; Temperature; Inert atmosphere;96.2%
With 1,10-Phenanthroline; ethylenediaminetetraacetic acid; sodium hydroxide In paraffin oil at 203 - 207℃; for 7h; Inert atmosphere;93.7%
With iron(III) chloride In 1,2-dichloro-ethane at 60℃; for 15h; Reagent/catalyst; Solvent; Temperature;93.9%
41481-63-4

4,4’-sulfonylbis((allyloxy)benzene)

A

3-allyl-4,4'-dihydroxydiphenyl sulfone

B

737795-84-5

3-allyl-4'-allyloxy-4-hydroxydiphenyl sulfone

C

5-(3-allyl-4-hydroxyphenylsulfonyl)-1-oxa-2-methylindane

D

41481-66-7

3,3′-diallyl-4,4′-dihydroxydiphenylsulfone

Conditions
ConditionsYield
With dmap at 160 - 280℃; for 0.0833333 - 0.333333h; Product distribution / selectivity; Microwave irradiation;
With 1,10-Phenanthroline; ascorbic acid In 1,2,3-trichlorobenzene at 210℃; for 7h; Product distribution / selectivity;
With 1,10-Phenanthroline; ascorbic acid at 160 - 280℃; for 0.266667h; Product distribution / selectivity; Microwave irradiation;
48%-caustic soda

48%-caustic soda

41481-63-4

4,4’-sulfonylbis((allyloxy)benzene)

41481-66-7

3,3′-diallyl-4,4′-dihydroxydiphenylsulfone

Conditions
ConditionsYield
With 1,2,3-trichlorobenzene In water14.0 parts (93.3%)
41481-63-4

4,4’-sulfonylbis((allyloxy)benzene)

122438-87-3

4,4’-sulfonylbis(2-allyl-1-(allyloxy)benzene)

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 4 h / 220 °C / Inert atmosphere
2.1: potassium carbonate / acetone / 1 h / Inert atmosphere; Reflux
2.2: Reflux; Inert atmosphere
View Scheme
41481-63-4

4,4’-sulfonylbis((allyloxy)benzene)

1636900-13-4

C32H42O8S5

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 4 h / 220 °C / Inert atmosphere
2.1: potassium carbonate / acetone / 1 h / Inert atmosphere; Reflux
2.2: Reflux; Inert atmosphere
3.1: 2,2'-azobis(isobutyronitrile) / tetrahydrofuran / 16.5 h / 20 - 65 °C / Inert atmosphere
View Scheme

1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene Specification

The Benzene,1,1'-sulfonylbis[4-(2-propen-1-yloxy)-, with CAS registry number 41481-63-4, belongs to the following product categories: (1)Industrial/Fine Chemicals; (2)Aromatics. It has the systematic name of 1,1'-sulfonylbis[4-(prop-2-en-1-yloxy)benzene]. And the chemical formula of this chemical is C18H18O4S.

Physical properties of Benzene,1,1'-sulfonylbis[4-(2-propen-1-yloxy)-: (1)ACD/LogP: 4.44; (2)# of Rule of 5 Violations: 0; (3)#H bond acceptors: 4; (4)#H bond donors: 0; (5)#Freely Rotating Bonds: 8; (6)Polar Surface Area: 60.98 Å2; (7)Index of Refraction: 1.559; (8)Molar Refractivity: 91.07 cm3; (9)Molar Volume: 282 cm3; (10)Polarizability: 36.1×10-24cm3; (11)Surface Tension: 40.8 dyne/cm; (12)Enthalpy of Vaporization: 74.02 kJ/mol; (13)Vapour Pressure: 1.15E-09 mmHg at 25°C.

You can still convert the following datas into molecular structure:
(1)SMILES: O=S(=O)(c1ccc(OC/C=C)cc1)c2ccc(OC\C=C)cc2
(2)InChI: InChI=1/C18H18O4S/c1-3-13-21-15-5-9-17(10-6-15)23(19,20)18-11-7-16(8-12-18)22-14-4-2/h3-12H,1-2,13-14H2
(3)InChIKey: JUNVYDTYJZSTKY-UHFFFAOYAT
(4)Std. InChI: InChI=1S/C18H18O4S/c1-3-13-21-15-5-9-17(10-6-15)23(19,20)18-11-7-16(8-12-18)22-14-4-2/h3-12H,1-2,13-14H2
(5)Std. InChIKey: JUNVYDTYJZSTKY-UHFFFAOYSA-N

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