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Cas Database |
| Name |
2-Fluoro-4-iodoaniline |
EINECS | N/A |
| CAS No. | 29632-74-4 | Density | 2.008 g/cm3 |
| PSA | 26.02000 | LogP | 2.59370 |
| Solubility | insoluble in water | Melting Point |
55-57 °C(lit.) |
| Formula | C6H5FIN | Boiling Point | 248.6 °C at 760 mmHg |
| Molecular Weight | 237.015 | Flash Point | 104.2 °C |
| Transport Information | N/A | Appearance | off-white to brown powder |
| Safety | 26-36-37/39-26/37/39 | Risk Codes | 36/37/38-20/21/22 |
| Molecular Structure |
|
Hazard Symbols |
 Xn,  T,  Xi
|
| Synonyms |
2-fluoro-4-iodin anline; |
Article Data | 8 |
2-Fluoro-4-iodoaniline Synthetic route
- 348-54-9
2-Fluoroaniline
- 29632-74-4
2-fluro-4-iodoaniline
Conditions
| Conditions | Yield |
|---|---|
| With iodine; sodium hydrogencarbonate In water at 60 - 80℃; for 2h; | 77% |
| With iodine; sodium hydrogencarbonate In water at 60℃; for 3h; | 76% |
| Stage #1: 2-Fluoroaniline With n-butyllithium In diethyl ether; hexane at -78℃; for 1h; Stage #2: With poly[4-(dibutyliodostannyl)butyl]styrene In diethyl ether; hexane at 20℃; for 18h; Stage #3: With Iodine monochloride In diethyl ether; hexane at -78 - 20℃; | 67% |
- 29632-74-4
2-fluro-4-iodoaniline
- 1066-54-2
trimethylsilylacetylene
- 518342-58-0
2-fluoro-4-((trimethylsilyl)ethynyl)aniline
Conditions
| Conditions | Yield |
|---|---|
| With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In tetrahydrofuran at 20℃; for 21h; Sonogashira Cross-Coupling; Inert atmosphere; | 100% |
| With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine at 20℃; Inert atmosphere; | 100% |
| With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide at 20℃; for 15h; Sonogashira Coupling; | 88% |
- 867130-26-5
4-chloro-1-methyl-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid
- 29632-74-4
2-fluro-4-iodoaniline
- 934664-24-1
4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylic acid
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 4-chloro-1-methyl-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid; 2-fluro-4-iodoaniline With lithium hexamethyldisilazane In tetrahydrofuran at 20℃; for 4h; Stage #2: With hydrogenchloride In tetrahydrofuran; water Product distribution / selectivity; | 100% |
| Stage #1: 4-chloro-1-methyl-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid; 2-fluro-4-iodoaniline With lithium hexamethyldisilazane In tetrahydrofuran at 20℃; for 4.08333h; Stage #2: With hydrogenchloride In tetrahydrofuran; water Product distribution / selectivity; | 100% |
| Stage #1: 4-chloro-1-methyl-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid; 2-fluro-4-iodoaniline With lithium hexamethyldisilazane In tetrahydrofuran at 20℃; for 4.08333h; Stage #2: With hydrogenchloride In tetrahydrofuran; water Product distribution / selectivity; | 100% |
- 463-71-8
thiophosgene
- 29632-74-4
2-fluro-4-iodoaniline
- 945530-32-5
2-fluoro-4-iodo-1-isothiocyanatobenzene
Conditions
| Conditions | Yield |
|---|---|
| In chloroform; water at 20℃; for 16h; | 100% |
| In chloroform; water at 20℃; for 16h; | 100% |
| In dichloromethane; water at 20℃; | 96.8% |
Conditions
| Conditions | Yield |
|---|---|
| With acetic anhydride In tetrahydrofuran; toluene at 20℃; | 100% |
- 29632-74-4
2-fluro-4-iodoaniline
- 140-90-9
sodium O-ethyl dithiocarbonate
- 54420-94-9
6-iodobenzo[d]thiazole-2-thiol
Conditions
| Conditions | Yield |
|---|---|
| In N,N-dimethyl-formamide at 95℃; for 5h; | 100% |
- 29632-74-4
2-fluro-4-iodoaniline
- 61079-72-9
2,3,4,-trifluorobenzoic acid
- 391211-97-5
3,4-difluoro-2-(2-fluoro-4-iodo-phenylamino)-benzoic acid
Conditions
| Conditions | Yield |
|---|---|
| With lithium amide In tetrahydrofuran | 99% |
| With lithium amide In N,N-dimethyl-formamide Inert atmosphere; | 85% |
| With lithium amide In tetrahydrofuran at 45 - 55℃; for 1.25 - 2.5h; Product distribution / selectivity; | 80% |
- 29632-74-4
2-fluro-4-iodoaniline
- 945559-14-8
1-azido-2-fluoro-4-iodobenzene
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 2-fluro-4-iodoaniline With trifluoroacetic acid; sodium nitrite at 0℃; for 0.5h; Stage #2: With sodium azide In water at 0℃; for 1h; | 99% |
| Stage #1: 2-fluro-4-iodoaniline With hydrogenchloride; sodium nitrite In water at -5℃; for 0.5h; Stage #2: With sodium azide In water at -5℃; for 1h; | 97% |
Conditions
| Conditions | Yield |
|---|---|
| With N,N`-dimethylethylenediamine; copper (I) trifluoromethane sulfonate benzene In dimethyl sulfoxide at 120℃; for 16h; | 99% |
| copper(I) trifluoromethanesulfonate benzene complex; N,N`-dimethylethylenediamine In dimethyl sulfoxide at 120℃; for 16h; | 99% |
| With N,N`-dimethylethylenediamine; copper(I) trifluoromethanesulfonate benzene In dimethyl sulfoxide at 120℃; for 16h; | 99% |
- 29632-74-4
2-fluro-4-iodoaniline
- 4023-34-1
cyclopropanecarboxylic acid chloride
- 1061683-60-0
N-(2-fluoro-4-iodophenyl)cyclopropanecarboxamide
Conditions
| Conditions | Yield |
|---|---|
| With triethylamine In tetrahydrofuran at 0 - 20℃; | 99% |
2-Fluoro-4-iodoaniline Chemical Properties
The Molecular formula of 2-Fluoro-4-iodoaniline(29632-74-4) : C6H5FIN
The Molecular Weight of 2-Fluoro-4-iodoaniline(29632-74-4) : 237.01
Molecular Structure :
Melting point: 55-57 °C(lit.)
Flash point: >230 °F
WATER Solubility: insoluble
Sensitive: Light Sensitive
Appearaance: light brown to brown Solid
Synonyms: 2-FLUORO-4-IODOBENZENAMINE;2-FLUORO-4-IODO-PHENYLAMINE;2-Fluoro-4-idioaniline;2-Fluoro-4-iodoaniline 98%;2-FLUORO-4-IODOANILINE;2-Fluoro-4-iodoaniline98%;
The Molecular Weight of 2-Fluoro-4-iodoaniline(29632-74-4) : 237.01
Molecular Structure :
Melting point: 55-57 °C(lit.)
Flash point: >230 °F
WATER Solubility: insoluble
Sensitive: Light Sensitive
Appearaance: light brown to brown Solid
Synonyms: 2-FLUORO-4-IODOBENZENAMINE;2-FLUORO-4-IODO-PHENYLAMINE;2-Fluoro-4-idioaniline;2-Fluoro-4-iodoaniline 98%;2-FLUORO-4-IODOANILINE;2-Fluoro-4-iodoaniline98%;
2-Fluoro-4-iodoaniline Safety Profile
The Hazard Codes of 2-Fluoro-4-iodoaniline(29632-74-4): 
Xi,Xn , 
T
The Risk Statements information of 2-Fluoro-4-iodoaniline(29632-74-4):
20/21/22: Harmful by inhalation, in contact with skin and if swallowed
36/37/38: Irritating to eyes, respiratory system and skin
The Safety Statements information of 2-Fluoro-4-iodoaniline(29632-74-4):
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
37/39: Wear suitable gloves and eye/face protection
36/37/39: Wear suitable protective clothing, gloves and eye/face protection
RIDADR: PG3
WGK Germany: 3
Hazard Note: Toxic
Xi,Xn , TThe Risk Statements information of 2-Fluoro-4-iodoaniline(29632-74-4):
20/21/22: Harmful by inhalation, in contact with skin and if swallowed
36/37/38: Irritating to eyes, respiratory system and skin
The Safety Statements information of 2-Fluoro-4-iodoaniline(29632-74-4):
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
37/39: Wear suitable gloves and eye/face protection
36/37/39: Wear suitable protective clothing, gloves and eye/face protection
RIDADR: PG3
WGK Germany: 3
Hazard Note: Toxic
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2-Fluoro-4-iodoaniline
