Basic Information | Post buying leads | Suppliers | Cas Database |
Conditions | Yield |
---|---|
With iodoform; sodium iodide In N,N-dimethyl-formamide for 3h; Catalytic behavior; Irradiation; | 91% |
With acetyl iodide at 80 - 90℃; for 1.5h; | 24% |
With iodine; aluminium |
(i-C3H7)3SbI2
A
2-iodo-propane
B
tri(isopropyl)antimony
C
diisopropylantimony iodide
Conditions | Yield |
---|---|
under Ar, decomposed at 135°C for 30 min; distd., not separated from triisopropyl stibine; elem. anal.; | A 89% B n/a C n/a |
Conditions | Yield |
---|---|
With 2-fluoro-2-(piperidin-1-yl)-4-(2,3,5,6-tetrafluoropyridin-4-yl)-5-(2,4,6-triisopropylphenyl)-1,3-dithiole In 1,4-dioxane at 45℃; for 14h; Schlenk technique; Inert atmosphere; | 74% |
Conditions | Yield |
---|---|
With N-iodo-succinimide In chlorobenzene for 3h; Irradiation; | A 51% B 18% |
Conditions | Yield |
---|---|
With CCl4*2AlI3 In dichloromethane at -20℃; for 1.5h; | 50% |
5'-O-(4,4'-dimethoxytrityl)-2-N-<2-<(tert-butyldiphenylsilyloxy)methyl>benzoyl>guanosine
tert-butyldimethylsilyl chloride
A
2-iodo-propane
B
5'-O-(4,4'-dimethoxytrityl)-3'-O-(tert-butyldimethylsilyl)-2-N-<2-<(tert-butyldiphenylsilyloxy)methyl>benzoyl>guanosine
Conditions | Yield |
---|---|
With pyridine; silver nitrate In tetrahydrofuran | A 42% B 16% |
Conditions | Yield |
---|---|
With water; hydrogen iodide |
propene
2-iodo-propane
Conditions | Yield |
---|---|
With hydrogen iodide | |
With ascaridole; hydrogen iodide | |
With hydrogen iodide; diphenylamine | |
With hydrogen iodide |
Conditions | Yield |
---|---|
With hydrogen iodide; diphenylamine |
Conditions | Yield |
---|---|
With hydrogen iodide |
1. | ihl-rat LC50:320,000 mg/m3/30M | FAVUAI Fiziologicheski Aktivnye Veshchestva. Physiologically Active Substances. 7 (1975),35. | ||
2. | ipr-mus LD50:1300 mg/kg | 34ZIAG Toxicology of Drugs and Chemicals ,Deichmann, W.B.,New York, NY.: Academic Press, Inc.,1969,756. |