cas 145100-51-2, 2-[N,N-BIS(TRIFLUOROMETHANESULFONYL)AMINO]-5-CHLOROPYRIDINE | Articles data ｜lookchem

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145100-51-2

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A metathesis-based approach to the synthesis of 2-pyridones and pyridines
(Chemical Equation Presented) The ring-closing metathesis reaction has been successfully employed to form a range of dihydropyridone intermediates, which are in the correct oxidation state to undergo a base-induced elimination to reveal the aromatic 2-pyridone. This mild and novel approach to six-membered heteroaromatic compounds then provides access to a wide variety of substituted pyridines in excellent overall yield.
Donohoe, Timothy J.,Fishlock, Lisa P.,Procopiou, Panayiotis A.
p. 285 - 288
(2008/09/19)

Synthesis of two conformationally constrained analogues of the minor tobacco alkaloid anabasine.
The anabasine analogues spiro[4-azaindan-1,2'-piperidine] (7) and spiro[6-azaindan-1,2'-piperidine] (8) have been prepared. A series of palladium-catalyzed reactions, where an intramolecular cyclization constituted a key reaction, were utilized for the pr
Lindstroem,Ripa,Hallberg
p. 2291 - 2293
(2007/10/03)

Pyridine-derived triflating reagents: N-(2-pyridyl)-triflimide and n-(5-chloro-2-pyridyl)triflimide
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Comins, Daniel L.,Dehghani, Ali,Foti, Christopher J.,Joseph, Sajan P.
p. 77 - 77
(2017/09/08)

Pyridine-Derived Triflating Reagents: An Improved Preparation of Vinyl Triflates from Metallo Enolates.
Metallo enolates of ketones are trapped with an N-(2-pyridyl)triflimide at low temperatures to give vinyl triflates.
Comins, Daniel L.,Dehghani, Ali
p. 6299 - 6302
(2007/10/02)

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Chemical Properties

Appearance/Colour :White to pale yellow crystalline solid
Melting Point: 45-47 °C(lit.)
Boiling Point: 358.316 °C at 760 mmHg
Flash Point:170.504 °C
Density: 1.893 g/c³
Solubility:Benzene (Slightly)
Storage Temp.:Keep Cold
Vapor Pressure: 13.9mmHg at 25°C
Refractive Index: 1.379
PKA: -7.71±0.10(Predicted)
Sensitive: Moisture Sensitive
BRN: 5833971
PSA: 101.17000
LogP: 4.40220

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