cas 60-38-8, 3-ACETYL STROPHANTHIDIN | Articles data ｜lookchem

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60-38-8

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SYNTHESIS OF STROPHANTHIDIN
A 16-step synthesis of strophanthidin (3) from a commercially available steroid 4 is described.Salient features of this approach are the selective reduction of the dienone system in 7 to give 8 and a one-pot introduction of 5β- and 14β-hydroxyls by addition of HOBr (14 -> 15).The stereo- and regioselectivity of the HOBr addition to the 5,6-double bond is controlled by 19-formyloxy group.
Kocovsky, Pavel,Stieborova, Irena
p. 4295 - 4298
(1989)
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Chemical Properties

Melting Point: 246-248℃
Boiling Point: 612.8 °C at 760 mmHg
Flash Point:205.7 °C
Density: 1.31 g/cm³
Storage Temp.:−20°C
PSA: 110.13000
LogP: 2.46900

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