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86061-04-3

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Synthesis of aryl esters of protected amino acids from aryl sulfonates
Aryl esters of Boc- and Fmoc-protected amino acids derived from electron-deficient phenols have been prepared in good yields from aryl 4- nitrobenzenesulfonates in the presence of 1-hydroxy-benzotriazole as catalyst.
Pudhom, Khanitha,Vilaivan, Tirayut
p. 5939 - 5942
(2007/10/03)

9-Fluorenylmethyl Pentafluorophenyl Carbonate as a Useful Reagent for the Preparation of N-9-Fluorenylmethyloxycarbonylamino Acids and their Pentafluorophenyl Esters
9-Fluorenylmethyl pentafluorophenyl carbonate is a useful reagent for the efficient, side reaction-free introduction of N-9-fluorenylmethyloxycarbonyl protecting group into amino acids and for the subsequent preparation of their pentafluorophenyl esters.Some new compounds of both types are described.
Schoen, Istvan,Kisfaludy, Lajos
p. 303 - 305
(2007/10/02)

Preparation and Applications of Pentafluorophenyl Esters of 9-Fluorenylmethyloxycarbonyl Amino Acids for Peptide Synthesis
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Kisfaludy, Lajos,Schoen, Istvan
p. 325 - 327
(2007/10/02)

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Chemical Properties

Melting Point: 119-120℃
Boiling Point: 674.2 °C at 760 mmHg
Flash Point:361.5 °C
Density: 1.352g/cm³
Storage Temp.:2-8°C
Vapor Pressure: 4.89E-18mmHg at 25°C
Refractive Index: 1.544
PKA: 10.08±0.46(Predicted)
BRN: 3642680
PSA: 90.93000
LogP: 6.70760

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