Silane, hexylphenyl-

Base Information

• Chemical Name: Silane, hexylphenyl-
• CAS No.: 4314-98-1
• Molecular Formula: C12H20Si
• Molecular Weight: 192.376
• Mol file: 4314-98-1.mol

Synonyms:Silane,hexylphenyl;C6H13SiH2Ph;hexyl-phenyl-silane;

Chemical Property of Silane, hexylphenyl-

Chemical Property:

• PSA: 0.00000
• LogP: 2.47930

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Silane, hexylphenyl-

There total 22 articles about Silane, hexylphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-hexene (592-41-6,25067-06-5) + phenylsilane (694-53-1) → hexyl-phenyl-silane (4314-98-1)

Guidance literature:

With C₄₂H₅₂Cl₂FeN₂; ethylmagnesium bromide; In tetrahydrofuran; toluene; at 25 ℃; for 24h; Temperature;

Reference yield: 94.0%

phenylchlorosilane (4206-75-1) → hexyl-phenyl-silane (4314-98-1)

Guidance literature:

In tetrahydrofuran; diethyl ether; at 30 ℃;

DOI:10.1039/b717717h

Reference yield: 94.0%

phenylchlorosilane (4206-75-1) + n-hexylmagnesium bromide (3761-92-0) → hexyl-phenyl-silane (4314-98-1)

Guidance literature:

In diethyl ether; at 30 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja206745w

upstream raw materials:

1-hexene

phenylsilane

bromo-phenyl-silane

trans-2-hexene

Refernces

• 1、 Keil, Philip M.,Hadlington, Terrance J.. "Geometrically Constrained Cationic Low-Coordinate Tetrylenes: Highly Lewis Acidic σ-Donor Ligands in Catalytic Systems". supporting information. . Retrieved 2022/01/13.
• 2、 Kraetschmer, Frederic,Roesky, Peter W.,Simler, Thomas,Sun, Xiaofei. "Thermally Stable Rare-Earth Metal Complexes Supported by Chelating Silylene Ligands". . p. 2100 - 2107. Retrieved 2021/07/20.