Technology Process of Magnesium chloride 2-phenylethyn-1-ide (1/1/1)
There total 1 articles about Magnesium chloride 2-phenylethyn-1-ide (1/1/1) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
isopropylmagnesium chloride;
In
tetrahydrofuran;
at 0 ℃;
Inert atmosphere of N2;
- Guidance literature:
-
With
[1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride;
In
1,2-dimethoxyethane;
at 85 ℃;
for 20h;
Schlenk technique;
Inert atmosphere;
DOI:10.1002/chem.201602315
- Guidance literature:
-
With
[1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride;
In
1,2-dimethoxyethane;
at 85 ℃;
for 20h;
Schlenk technique;
Inert atmosphere;
DOI:10.1002/chem.201602315