Hydroxylamine, hydrofluoride

Base Information

• Chemical Name: Hydroxylamine, hydrofluoride
• CAS No.: 17256-78-9
• Molecular Formula: FH . H3 N O
• Molecular Weight: 53.0363
• European Community (EC) Number: 241-291-6
• DSSTox Substance ID: DTXSID9066178
• Mol file: 17256-78-9.mol

Synonyms:Hydroxylamine, hydrofluoride;Hydroxylamine hydrofluoride;17256-78-9;hydroxylamine;hydrofluoride;Hydroxylammonium fluoride;EINECS 241-291-6;Hydroxylamine, hydrofluoride (1:1);FH.H3NO;F-H.H3-N-O;DTXSID9066178

Chemical Property of Hydroxylamine, hydrofluoride

Chemical Property:

• Vapor Pressure: 179mmHg at 25°C
• Boiling Point: 56.5°Cat760mmHg
• Flash Point: °C
• PSA: 46.25000
• Density: g/cm³
• LogP: 0.56730
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 53.027691913
• Heavy Atom Count: 3
• Complexity: 2

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: NO.F

Technology Process of Hydroxylamine, hydrofluoride

There total 3 articles about Hydroxylamine, hydrofluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

perchloryl fluoride (7616-94-6) + hydroxylamine (7803-49-8) → hydroxylamine nitrate (13465-08-2) + hydroxylammonium fluoride (17256-78-9,68110-20-3)

Guidance literature:

In ethanol; -70 to -60°C, storing (120 h), gradual increase of temperature; IR spectroscopy;

Reference yield:

hydrogen fluoride (7664-39-3,12381-92-9,32057-09-3,74835-82-8) + hydroxylamine hydrochloride (5470-11-1) → hydroxylammonium fluoride (17256-78-9,68110-20-3)

Guidance literature:

hydroxylamine hydrochloride; With sodium ethanolate;

hydrogen fluoride; In water; at 0 ℃;

Reference yield:

perchloryl fluoride (7616-94-6) + hydroxylamine (7803-49-8) → hydroxylammonium fluoride (17256-78-9,68110-20-3) + hydroxylammonium chlorate (66857-72-5)

Guidance literature:

In ethanol; hydroxylamine soln. freezing and evac. (vac. apparatus), calculated amount of ClO3F addmitting (condn. in reaction flask), reaction mixt. keeping without or with stirring for definite time at given temp. until complete removal of volatile substances; no isolation of individual substances; chem. anal., IR spectroscopy;

upstream raw materials:

perchloryl fluoride

hydroxylamine

hydrogen fluoride

hydroxylamine hydrochloride

Refernces

• 1、 Kristl, Matja?,Dojer, Brina,Hojnik, Nu?a,Golobi?, Amalija. "Synthesis and characterization of new hydroxylammonium fluoromanganates and fluoroscandates". . p. 15 - 21. Retrieved 2014/12/11.
• 2、 Titova, K. V.,Loginova, E. N.. "Reactions of ClO3F and Cl2O7 with Some Amines". . p. 1714 - 1720. Retrieved 2008/10/08.