Technology Process of Cyclopropaneacetic acid, 1-[(methylsulfonyl)oxy]-, phenylmethyl ester
There total 6 articles about Cyclopropaneacetic acid, 1-[(methylsulfonyl)oxy]-, phenylmethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Et3N; DMAP / CH2Cl2 / 4 h / 20 °C
2: 57.0 g / oxone / tetrahydrofuran; H2O / 8 h / 20 °C
3: 83 percent / p-TsOH hydrate / toluene / 6 h / Heating
With
dmap; Oxone; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1002/adsc.200404025
- Guidance literature:
-
Multi-step reaction with 3 steps
1: aq. HCl / tetrahydrofuran / 0.5 h / 0 °C
2: 14.6 g / aq. H2O2 / tetrahydrofuran / 8 h / 60 °C
3: 83 percent / p-TsOH hydrate / toluene / 6 h / Heating
With
hydrogenchloride; dihydrogen peroxide; toluene-4-sulfonic acid;
In
tetrahydrofuran; toluene;
DOI:10.1002/adsc.200404025