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2-(BOC-AMINO)-5-PICOLINE

Base Information Edit
  • Chemical Name:2-(BOC-AMINO)-5-PICOLINE
  • CAS No.:562074-43-5
  • Molecular Formula:C11H16N2O2
  • Molecular Weight:208.26
  • Hs Code.:2933399090
  • Mol file:562074-43-5.mol
2-(BOC-AMINO)-5-PICOLINE

Synonyms:Carbamicacid, (5-methyl-2-pyridinyl)-, 1,1-dimethylethyl ester (9CI);

Suppliers and Price of 2-(BOC-AMINO)-5-PICOLINE
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • Labseeker
  • Carbamicacid,N-(5-methyl-2-pyridinyl)-,1,1-dimethylethylester 95
  • 10g
  • $ 1925.00
  • Crysdot
  • tert-Butyl(5-methylpyridin-2-yl)carbamate 95+%
  • 5g
  • $ 158.00
  • Crysdot
  • tert-Butyl(5-methylpyridin-2-yl)carbamate 95+%
  • 25g
  • $ 380.00
  • Chemenu
  • tert-butyl(5-methylpyridin-2-yl)carbamate 95%
  • 25g
  • $ 320.00
  • Chemenu
  • tert-butyl(5-methylpyridin-2-yl)carbamate 95%
  • 100g
  • $ 746.00
  • American Custom Chemicals Corporation
  • 2-(BOC-AMINO)-5-PICOLINE 95.00%
  • 5MG
  • $ 504.93
  • Alichem
  • tert-Butyl(5-methylpyridin-2-yl)carbamate
  • 100g
  • $ 805.98
  • AK Scientific
  • 2-(BOC-Amnio)-5-methylpyridine
  • 100g
  • $ 1111.00
  • AK Scientific
  • 2-(BOC-Amnio)-5-methylpyridine
  • 25g
  • $ 471.00
  • AK Scientific
  • 2-(BOC-Amnio)-5-methylpyridine
  • 5g
  • $ 191.00
Total 14 raw suppliers
Chemical Property of 2-(BOC-AMINO)-5-PICOLINE Edit
Chemical Property:
  • Boiling Point:273.7 °C at 760 mmHg 
  • Flash Point:119.3 °C 
  • PSA:51.22000 
  • Density:1.108 g/cm3 
  • LogP:2.81000 
  • Storage Temp.:2-8°C 
Purity/Quality:

98%Min *data from raw suppliers

Carbamicacid,N-(5-methyl-2-pyridinyl)-,1,1-dimethylethylester 95 *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of 2-(BOC-AMINO)-5-PICOLINE

There total 2 articles about 2-(BOC-AMINO)-5-PICOLINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In tetrahydrofuran; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.joc.6b01324
Guidance literature:
With (1,2-dimethoxyethane)dichloronickel(II); (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; 4,4'-di-tert-butyl-2,2'-bipyridine; N,N,N',N'-tetramethylguanidine; In acetonitrile; at 23 ℃; for 48h; Inert atmosphere; Irradiation;
DOI:10.1021/acs.joc.8b02182
Guidance literature:
Multi-step reaction with 5 steps
1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 1.5 h / Reflux
2: caesium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C
3: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 50 °C / Argon
4: triethylamine / dichloromethane / 16 h / 20 °C
5: hydrogenchloride / 1,4-dioxane; methanol / 22 h / 20 °C
With hydrogenchloride; N-Bromosuccinimide; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); caesium carbonate; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;
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