1,5-Diphenyl-3-pentanone

Base Information

• Chemical Name: 1,5-Diphenyl-3-pentanone
• CAS No.: 5396-91-8
• Molecular Formula: C17H18O
• Molecular Weight: 238.329
• Hs Code.: 2914399090
• NSC Number: 10969,4397
• DSSTox Substance ID: DTXSID10202250
• Nikkaji Number: J99.761G
• Wikidata: Q69756377
• ChEMBL ID: CHEMBL4173723
• Mol file: 5396-91-8.mol

Synonyms:1,5-diphenylpentan-3-one;1,5-DIPHENYL-3-PENTANONE;5396-91-8;Diphenethyl ketone;Dibenzylacetone;3-Pentanone, 1,5-diphenyl-;3-Pentanone,5-diphenyl-;NSC4397;1,5diphenyl-3-pentanone;1,5-diphenyl-pentan-3-one;SCHEMBL497371;1,5-di-(phenyl)-3-pentanone;CHEMBL4173723;DTXSID10202250;AMY30958;NSC 4397;NSC-4397;NSC10969;NSC 10969;NSC-10969;STL444352;AKOS010644454;CS-0231127;EN300-107168;Z815261606

Chemical Property of 1,5-Diphenyl-3-pentanone

Chemical Property:

• Vapor Pressure: 3.95E-05mmHg at 25°C
• Melting Point: 13.5°C
• Refractive Index: 1.559
• Boiling Point: 352 °C at 760 mmHg
• Flash Point: 153.7 °C
• PSA: 17.07000
• Density: 1.038 g/cm³
• LogP: 3.82110
• XLogP3: 3.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 6
• Exact Mass: 238.135765193
• Heavy Atom Count: 18
• Complexity: 210

Purity/Quality:

99% ^*data from raw suppliers

1,5-Diphenyl-3-pentanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)CCC(=O)CCC2=CC=CC=C2

Technology Process of 1,5-Diphenyl-3-pentanone

There total 93 articles about 1,5-Diphenyl-3-pentanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

dibenzylideneacetone (35225-79-7) → 1,5-diphenyl-3-pentanone (5396-91-8)

Guidance literature:

With zinc copper; In methanol; water; for 5h; Heating;

Reference yield: 93.0%

4-Phenyl-2-butanone (2550-26-7) + benzyl alcohol (100-51-6,185532-71-2) → 1,5-diphenyl-3-pentanone (5396-91-8)

Guidance literature:

With barium hydroxide monohydrate; water; palladium nanoparticles in poly(viologen); at 100 ℃; for 24h;

DOI:10.1021/ol060166q

Reference yield: 91.0%

acetone (67-64-1) + benzyl alcohol (100-51-6,185532-71-2) → 1,5-diphenyl-3-pentanone (5396-91-8)

Guidance literature:

With trifuran-2-yl-phosphane; C₄₈H₃₄F₆N₄O₄Pd₂; lithium hydroxide; In neat (no solvent); at 80 - 100 ℃; for 24h; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1021/acs.organomet.7b00478

upstream raw materials:

(E)-1,5-diphenyl-1-penten-4-yn-3-one

dibenzylideneacetone

1,5-diphenyl-1-penten-3-one

1,5?diphenylpenta?1,4?dien?3?one oxime

Downstream raw materials:

3-phenethyl-1,5-diphenyl-pentan-3-ol

1,5-diphenylpentan-3-ol

1,5-diphenylpentane

1,5-diphenyl-pentan-3-one oxime

Refernces

• 1、 Charushin, V. N.,Chupakhin, O. N.,Gorbunov, E. B.,Grzhegorzhevskii, K. V.,Kovalev, I. S.,Minin, A. S.,Sadieva, L. K.,Taniya, O. S.,Tsurkan, M. V.,Volkova, N. N.,Zyryanov, G. V.. "Bola-type PAH-based fluorophores/chemosensors: Synthesis via an unusual clemmensen reduction and photophysical studies". . . Retrieved 2021/08/21.
• 2、 Wang, Feng,Wang, Min,Zhang, Zhe,Zhou, Hongru. "Surface Sulfate Ion on CdS Catalyst Enhances Syngas Generation from Biopolyols". . p. 6533 - 6541. Retrieved 2021/05/29.