AKOS BB-9729

Base Information

• Chemical Name: AKOS BB-9729
• CAS No.: 42194-25-2
• Molecular Formula: C13H23N
• Molecular Weight: 193.332
• Hs Code.: 2921300090
• Mol file: 42194-25-2.mol

Synonyms:D 191;3,5,7-Trimethyl-adamantan-1-ylamine;

Chemical Property of AKOS BB-9729

Chemical Property:

• Vapor Pressure: 0.0248mmHg at 25°C
• Boiling Point: 248°Cat760mmHg
• PKA: 10.81±0.70(Predicted)
• Flash Point: 92.5°C
• PSA: 26.02000
• Density: 1.039g/cm³
• LogP: 3.78450

Purity/Quality:

99%, ^*data from raw suppliers

3,5,7-Trimethyl-adamantan-1-ylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of AKOS BB-9729

There total 1 articles about AKOS BB-9729 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-trimethyladamantane (707-35-7) → 3,5,7-trimethyl-1-adamantanamine (42194-25-2)

Guidance literature:

Multi-step reaction with 4 steps

1: nitric acid / acetic acid

2: acetic acid / 90 °C

3: acetic acid; nitric acid / 90 °C

4: sodium hydroxide

With nitric acid; acetic acid; sodium hydroxide; In acetic acid;

DOI:10.1134/S1070428015120064

Reference yield:

1-Fluoro-2-isocyanato-benzene (16744-98-2) + 3,5,7-trimethyl-1-adamantanamine (42194-25-2) → 1-[3,5,7-trimethyl(adamantan-1-yl)]-3-(2-fluorophenyl) urea

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 8h;

DOI:10.1016/j.jfluchem.2019.02.005

Reference yield:

(rac)-1-(2-chloro-benzenesulfonyl)-piperidine-3-carboxylic acid (630049-60-4) + 3,5,7-trimethyl-1-adamantanamine (42194-25-2) → 1-(2-chloro-benzenesulfonyl)-piperidine-3-carboxylic acid (3,5,7-trimethyl-adamantan-1-yl)-amide (1057284-29-3)

Guidance literature:

With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 24h;

upstream raw materials:

1,3,5-trimethyladamantane

Downstream raw materials:

1-(2-chloro-benzenesulfonyl)-piperidine-3-carboxylic acid (3,5,7-trimethyl-adamantan-1-yl)-amide

3,5,7-trimethyl-1-aminoadamantane hydrochloride

Refernces