Technology Process of Tricyclo[3.3.1.13,7]decan-1-amine, 3,5,7-trimethyl-, hydrochloride
There total 7 articles about Tricyclo[3.3.1.13,7]decan-1-amine, 3,5,7-trimethyl-, hydrochloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: phosphoric acid / 17.5 h / 20 - 87 °C
1.2: 20 - 45 °C / pH 6 - 7
2.1: potassium hydroxide; butan-1-ol / 15.33 - 15.5 h / 20 - 132 °C
2.2: 0.33 h / 20 - 50 °C / pH 1
With
potassium hydroxide; phosphoric acid; butan-1-ol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: nitric acid / acetic acid
2: acetic acid / 90 °C
3: acetic acid; nitric acid / 90 °C
4: sodium hydroxide
5: hydrogenchloride
With
hydrogenchloride; nitric acid; acetic acid; sodium hydroxide;
In
acetic acid;
DOI:10.1134/S1070428015120064
- Guidance literature:
-
N-acetyl-3,5,7-trimethyl-1-aminoadamantane;
With
potassium hydroxide; butan-1-ol;
at 20 - 132 ℃;
for 15.33 - 15.5h;
With
hydrogenchloride;
In
water;
at 20 - 50 ℃;
for 0.333333h;
pH=1;