N-heptylaniline

Base Information

• Chemical Name: N-heptylaniline
• CAS No.: 3007-70-3
• Molecular Formula: C13H21 N
• Molecular Weight: 191.316
• Hs Code.: 2921420090
• Mol file: 3007-70-3.mol

Synonyms:Heptylamine,N-phenyl- (6CI,7CI,8CI); N-Heptylaniline; NSC 79262

Chemical Property of N-heptylaniline

Chemical Property:

• Vapor Pressure: 0.00173mmHg at 25°C
• Boiling Point: 293.4°Cat760mmHg
• PKA: 5.05±0.50(Predicted)
• Flash Point: 131.5°C
• PSA: 12.03000
• Density: 0.92g/cm³
• LogP: 4.14190

Purity/Quality:

99% ^*data from raw suppliers

N-HEPTYLANILINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-heptylaniline

There total 26 articles about N-heptylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

n-heptan1ol (111-70-6) + aniline (62-53-3) → N-(heptyl)aniline (3007-70-3)

Guidance literature:

With (4-Ph)Triaz(NHPⁱPr₂)₂Mn(CO)₂Br; potassium tert-butylate; In tetrahydrofuran; at 80 ℃; for 18h;

DOI:10.1021/acscatal.8b02530

Reference yield: 93.0%

1-Bromoheptane (629-04-9) + aniline (62-53-3) → N-(heptyl)aniline (3007-70-3)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 80 ℃; for 15h;

DOI:10.1080/00397919908086201

Reference yield: 92.0%

1-Heptylamine (111-68-2) + phenylboronic acid (98-80-6) → N-(heptyl)aniline (3007-70-3)

Guidance literature:

With copper-exchanged fluorapatite; In methanol; at 20 ℃; for 4h;

DOI:10.1021/jo0614036

upstream raw materials:

heptanal

nitrobenzene

aniline

1-Bromoheptane

Downstream raw materials:

4-heptylaniline

aniline

N-heptyl-N-methylaniline

N-(4-heptylphenyl)acetamide

Refernces

• 1、 Liu, Lin,Li, Wenxiu,Qi, Ran,Zhu, Qingqing,Li, Jing,Fang, Yuzhen,Kong, Xiangjin. "Cobalt encapsulated in N?doped graphene sheet for one-pot reductive amination to synthesize secondary amines". . . Retrieved 2021/03/14.
• 2、 Ma, Ruixuan,Qin, Jianhua,Shi, Lei,Zhang, Xinhai. "A base-free Chan–Lam reaction catalyzed by an easily assembled Cu(II)-carboxylate metal-organic framework". . p. 795 - 799. Retrieved 2021/07/06.