15-Hexadecenoic acid

Base Information

• Chemical Name: 15-Hexadecenoic acid
• CAS No.: 4675-57-4
• Molecular Formula: C16H30O2
• Molecular Weight: 254.413
• Mol file: 4675-57-4.mol

Synonyms:

Chemical Property of 15-Hexadecenoic acid

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 15-Hexadecenoic acid

There total 1 articles about 15-Hexadecenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-chloro-valeric acid (1119-46-6) + 10-undecenylmagnesium chloride (108712-21-6) → 15-hexadecenoic acid (4675-57-4) + 1-undecene (821-95-4) + 1,21-docosadiene (53057-53-7) + valeric acid (109-52-4)

Guidance literature:

With dilithium tetrachlorocuprate; ethylmagnesium bromide; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, Et₂O, -20 deg C, 20 min, 2.) -20 deg C, 1.5 h;

DOI:10.1021/jo00269a038

Reference yield:

15-hexadecenoic acid (4675-57-4) → 15-hexadecanolide (109-29-5)

Guidance literature:

Multi-step reaction with 2 steps

1: petroleum ether; dibenzoyl peroxide; hydrogen bromide

2: potassium carbonate; butanone

With hydrogen bromide; potassium carbonate; butanone; Petroleum ether; dibenzoyl peroxide;

Reference yield:

15-hexadecenoic acid (4675-57-4) → 16-bromohexadecanoic acid (2536-35-8)

Guidance literature:

With hydrogen bromide; Petroleum ether; dibenzoyl peroxide;

upstream raw materials:

5-chloro-valeric acid

10-undecenylmagnesium chloride

Downstream raw materials:

16-bromohexadecanoic acid

pentadecanedioic acid

15-hexadecanolide

Refernces