Technology Process of Benzenamine,
4-[2-(5-methoxy-3,3-dimethyl-3H-indol-2-yl)ethenyl]-N,N-dimethyl-
There total 1 articles about Benzenamine,
4-[2-(5-methoxy-3,3-dimethyl-3H-indol-2-yl)ethenyl]-N,N-dimethyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
5-Methoxy-2,3,3-trimethyl-3H-indole;
With
hydrogen bromide; acetic acid;
In
ethanol;
for 15h;
Heating;
4-dimethylamino-benzaldehyde;
With
trifluoroacetic acid;
In
ethanol; acetonitrile;
for 24h;
Heating;
DOI:10.1021/jp107116d
- Guidance literature:
-
With
boron tribromide;
In
dichloromethane;
at 0 - 20 ℃;
for 13h;
DOI:10.1021/jp107116d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: boron tribromide / dichloromethane / 13 h / 0 - 20 °C
2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 48 h / 0 - 20 °C
With
dmap; boron tribromide; dicyclohexyl-carbodiimide;
In
dichloromethane;
DOI:10.1021/jp107116d
