C10E3

Base Information

• Chemical Name: C10E3
• CAS No.: 4669-23-2
• Molecular Formula: C16H34 O4
• Molecular Weight: 290.444
• Mol file: 4669-23-2.mol

Synonyms:2-[2-(2-Decyloxyethoxy)ethoxy]ethanol;3,6,9-Trioxanonadecan-1-ol; C10E3; C10EO3; Nikkol BD 3SY; Triethylene glycolmonodecyl ether

Chemical Property of C10E3

Chemical Property:

• Refractive Index: n20/D 1.449
• Boiling Point: 383.1±22.0 °C(Predicted)
• PKA: 14.36±0.10(Predicted)
• PSA: 47.92000
• Density: 0.936 g/mL at 20oC(lit.)
• LogP: 3.16920
• Storage Temp.: 2-8°C

Purity/Quality:

98%Min ^*data from raw suppliers

Triethylene Glycol Monodecyl Ether ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: Triethylene Glycol Monodecyl Ether is a non-ionic surfactant.

Technology Process of C10E3

There total 1 articles about C10E3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

caprinaldehyde (112-31-2) + 2,2'-[1,2-ethanediylbis(oxy)]bisethanol (112-27-6) → 1-Decanol (112-30-1) + triethylene glycol mono-n-decyl ether (4669-23-2)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In 2,2'-[1,2-ethanediylbis(oxy)]bisethanol; at 200 ℃; for 3h; under 51716.2 Torr; Inert atmosphere;

Reference yield:

2-sulfobenzoic acid cyclic anhydride (81-08-3) + triethylene glycol mono-n-decyl ether (4669-23-2) → C23H38O8S

Guidance literature:

With dmap; In acetonitrile; at 20 - 80 ℃; for 3h;

DOI:10.1002/rcm.4367

Reference yield:

triethylene glycol mono-n-decyl ether (4669-23-2) → 3,4-bis-{2-[2-(2-decyloxy-ethoxy)-ethoxy]-ethoxy}-benzaldehyde (656821-30-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / PBr₃ / dioxane / 4 h / Heating

2: 70 percent / K₂CO₃ / dimethylformamide / 4 h / Heating

With phosphorus tribromide; potassium carbonate; In 1,4-dioxane; N,N-dimethyl-formamide;

DOI:10.1016/j.cplett.2003.09.150

upstream raw materials:

caprinaldehyde

2,2'-[1,2-ethanediylbis(oxy)]bisethanol

Downstream raw materials:

3,4-bis-{2-[2-(2-decyloxy-ethoxy)-ethoxy]-ethoxy}-benzaldehyde

Refernces

• 1、 -. "POLYOL ETHERS AND PROCESS FOR MAKING THEM". Page/Page column 8. . Retrieved 2010/03/31.