(Dimethylsilylene)bismethanol diacetate

Base Information

• Chemical Name: (Dimethylsilylene)bismethanol diacetate
• CAS No.: 2917-61-5
• Molecular Formula: C₈H₁₆O₄Si
• Molecular Weight: 204.298
• Mol file: 2917-61-5.mol

Synonyms:(Dimethylsilylene)bismethanol diacetate

Chemical Property of (Dimethylsilylene)bismethanol diacetate

Chemical Property:

• Boiling Point: 55 °C (0.150015 mmHg)
• PSA: 52.60000
• LogP: 1.73600

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (Dimethylsilylene)bismethanol diacetate

There total 5 articles about (Dimethylsilylene)bismethanol diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

bis(chloromethyl)dimethylsilane (2917-46-6) + sodium acetate (127-09-3) → Bis-acetoxymethyl-dimethyl-silan (2917-61-5)

Guidance literature:

In N,N-dimethyl-formamide; at 100 ℃; for 5h;

DOI:10.1039/c6ra19352h

Reference yield: 90.0%

bis(chloromethyl)dimethylsilane (2917-46-6) + potassium acetate (127-08-2) → Bis-acetoxymethyl-dimethyl-silan (2917-61-5)

Guidance literature:

In not given;

DOI:10.1021/ja01184a032

Reference yield:

bis(chloromethyl)dimethylsilane (2917-46-6) + acetic acid (64-19-7,77671-22-8) → Bis-acetoxymethyl-dimethyl-silan (2917-61-5)

Guidance literature:

With potassium acetate;

DOI:10.1021/jm00329a012

upstream raw materials:

bis(chloromethyl)dimethylsilane

sodium acetate

acetic acid

potassium acetate

Refernces

• 1、 Karimata, Ayumu,Matsumoto, Kozo,Endo, Takeshi. "Synthesis and characterization of polyurethanes bearing carbosilane segments". . p. 94803 - 94808. Retrieved 2016.
• 2、 Axthammer, Quirin J.,Klap?tke, Thomas M.,Krumm, Burkhard,Reith, Thomas. "Energetic Sila-Nitrocarbamates: Silicon Analogues of Neo-Pentane Derivatives". . p. 4683 - 4692. Retrieved 2016/05/24.
• 3、 Fessenden,Coon. "Silicon-substituted medicinal agents. Silacarbamates related to meprobamate.". . p. 604 - 608. Retrieved 2007/10/05.