Bis-(2,2,6,6-tetramethyl-piperidin-1-yl)-diazene

Base Information

• Chemical Name: Bis-(2,2,6,6-tetramethyl-piperidin-1-yl)-diazene
• CAS No.: 42053-22-5
• Molecular Formula: C₁₈H₃₆N₄
• Molecular Weight: 308.511
• Mol file: 42053-22-5.mol

Synonyms:Bis-(2,2,6,6-tetramethyl-piperidin-1-yl)-diazene

Chemical Property of Bis-(2,2,6,6-tetramethyl-piperidin-1-yl)-diazene

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of Bis-(2,2,6,6-tetramethyl-piperidin-1-yl)-diazene

There total 1 articles about Bis-(2,2,6,6-tetramethyl-piperidin-1-yl)-diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-amino-2,2,6,6-tetramethylpiperidine (6130-92-3) → 2,6-dimethyl-2-heptene (5557-98-2) + 2,6-dimethyl-1-heptene (3074-78-0) + Bis-(2,2,6,6-tetramethyl-piperidin-1-yl)-diazene (42053-22-5) + 1,1,3-trimethylcyclohexane (3073-66-3,150927-19-8,150927-30-3)

Guidance literature:

With tert-butylhypochlorite; triethylamine; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given; 1.) Et₂O, -78 degC, 1 h, 2.) CCl₃F, irradiation, 12 h;

DOI:10.1021/ja00388a031

upstream raw materials:

1-amino-2,2,6,6-tetramethylpiperidine

Refernces