Technology Process of Mirosamicina
There total 3 articles about Mirosamicina which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triphenylphosphine;
In
dichloromethane;
at 55 ℃;
for 67h;
DOI:10.1039/P19890000787
- Guidance literature:
-
With
multifunctional biosynthetic P450 monooxygenase; rhodococcus reductase domain; NADPH;
In
aq. buffer;
at 28 ℃;
for 2h;
pH=7.3;
Reagent/catalyst;
Kinetics;
Enzymatic reaction;
DOI:10.1021/ja4130302
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 39 percent / MCPBA, disodium hydrogen phosphate / CH2Cl2 / 23 h / 60 °C
2: 56 percent / triphenylphosphine / CH2Cl2 / 67 h / 55 °C
With
disodium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine;
In
dichloromethane;
DOI:10.1039/P19890000787