Technology Process of C19H21ClN5O2P
There total 5 articles about C19H21ClN5O2P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iron; ammonium chloride;
In
tetrahydrofuran; water;
at 65 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium phosphate / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / N,N-dimethyl-formamide / 3 h / 150 °C
2: potassium carbonate / N,N-dimethyl-formamide / 5 h / 60 °C
3: ammonia / methanol / 72 h / 100 °C / Sealed tube
4: potassium phosphate / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / N,N-dimethyl-formamide / 120 °C / Sealed tube
5: ammonium chloride; iron / water; tetrahydrofuran / 65 °C
With
potassium phosphate; ammonia; iron; potassium carbonate; ammonium chloride;
palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 60 °C
2: ammonia / methanol / 72 h / 100 °C / Sealed tube
3: potassium phosphate / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / N,N-dimethyl-formamide / 120 °C / Sealed tube
4: ammonium chloride; iron / water; tetrahydrofuran / 65 °C
With
potassium phosphate; ammonia; iron; potassium carbonate; ammonium chloride;
palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;