Technology Process of C60H85NO3Si2
There total 4 articles about C60H85NO3Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine;
In
tetrahydrofuran;
at 50 ℃;
for 18h;
DOI:10.1021/ma1016242
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 70 °C
2.1: hydrazine hydrate / ethanol / Reflux
2.2: 20 °C
2.3: 20 °C
3.1: triethylamine / N,N-dimethyl-formamide / 20 °C
4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 18 h / 50 °C
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; hydrazine hydrate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
1.1: Williamson synthesis / 4.1: Sonogashira-Hagihara coupling;
DOI:10.1021/ma1016242
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrazine hydrate / ethanol / Reflux
1.2: 20 °C
1.3: 20 °C
2.1: triethylamine / N,N-dimethyl-formamide / 20 °C
3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 18 h / 50 °C
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydrazine hydrate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
3.1: Sonogashira-Hagihara coupling;
DOI:10.1021/ma1016242