Technology Process of C9H11N3O4
There total 5 articles about C9H11N3O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrazine / dichloromethane / 2 h / 0 °C
2: hydroxylamine hydrochloride; sodium hydroxide / methanol / 20 °C
With
hydroxylamine hydrochloride; sodium hydroxide; hydrazine;
In
methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.01.134
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 60 °C
2.1: sodium chlorite; sodium dihydrogenorthophosphate; dihydrogen peroxide / water; acetonitrile / 20 °C / Cooling with ice
2.2: Cooling with ice
3.1: 4-methyl-morpholine / dichloromethane / 1 h / 0 °C
4.1: hydrazine / dichloromethane / 2 h / 0 °C
5.1: hydroxylamine hydrochloride; sodium hydroxide / methanol / 20 °C
With
4-methyl-morpholine; sodium chlorite; sodium dihydrogenorthophosphate; hydroxylamine hydrochloride; dihydrogen peroxide; potassium carbonate; sodium hydroxide; hydrazine;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.01.134