Technology Process of Dichloroisoproterenol
There total 3 articles about Dichloroisoproterenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
isopropylamine; 2-(3,4-dichlorophenyl)-2-oxoacetaldehyde;
In
1,2-dichloro-ethane;
at 25 ℃;
for 2h;
With
sodium tetrahydroborate;
In
1,2-dichloro-ethane;
at 0 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrachlorosilane; N,N,N,N,N,N-hexamethylphosphoric triamide / dichloromethane / 4 h / -20 °C / Inert atmosphere
2: ammonia borane / dichloromethane / 3 h / -20 - 20 °C / Inert atmosphere
With
N,N,N,N,N,N-hexamethylphosphoric triamide; ammonia borane; tetrachlorosilane;
In
dichloromethane;
1: |Passerini Condensation;
DOI:10.1002/chem.201500210
- Guidance literature:
-
With
ammonia borane;
In
dichloromethane;
at -20 - 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1002/chem.201500210
