Technology Process of di-(2-(bis(2,4,6-trimethylbenzoyl)phosphoryl)ethyl)sulfone
There total 3 articles about di-(2-(bis(2,4,6-trimethylbenzoyl)phosphoryl)ethyl)sulfone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide;
In
water; toluene;
at 20 ℃;
for 12h;
Inert atmosphere;
Schlenk technique;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / 1,2-dimethoxyethane; toluene / 12 h / 20 °C / Schlenk technique; Inert atmosphere
2: dihydrogen peroxide / toluene; water / 12 h / 20 °C / Inert atmosphere; Schlenk technique
With
dihydrogen peroxide; triethylamine;
In
1,2-dimethoxyethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium; phosphorus; ammonia; tert-butyl alcohol / 1,2-dimethoxyethane / 1 h / 20 °C / Schlenk technique; Inert atmosphere
2: hydrogenchloride / diethyl ether
3: triethylamine / 1,2-dimethoxyethane; toluene / 12 h / 20 °C / Schlenk technique; Inert atmosphere
4: dihydrogen peroxide / toluene; water / 12 h / 20 °C / Inert atmosphere; Schlenk technique
With
hydrogenchloride; phosphorus; ammonia; dihydrogen peroxide; sodium; triethylamine; tert-butyl alcohol;
In
1,2-dimethoxyethane; diethyl ether; water; toluene;
