Technology Process of (Dimethylamine)trihydroboron
There total 47 articles about (Dimethylamine)trihydroboron which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
neat (no solvent);
excess amine, 30-40°C, concn. of soln.;; distn. in vac. (60°C/2Torr) or recrystn. (petroleum ether);;
- Guidance literature:
-
With
iodine;
In
1,2-dimethoxyethane;
byproducts: NaI, H2; dropwise addn. of NaBH4 and I2 in DME to amine in DME, removal of solvent, addn. of C6H6, filtration, evapn. of filtrate in a N2 stream, drying in vac.;; recrystn. from CH2Cl2/hexane mixture;;