1-benzyl-2-propyldisulfane

Base Information

• Chemical Name: 1-benzyl-2-propyldisulfane
• CAS No.: 27657-11-0
• Molecular Formula: C₁₀H₁₄S₂
• Molecular Weight: 198.353
• Mol file: 27657-11-0.mol

Synonyms:1-benzyl-2-propyldisulfane

Chemical Property of 1-benzyl-2-propyldisulfane

Chemical Property:

Purity/Quality:

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Technology Process of 1-benzyl-2-propyldisulfane

There total 6 articles about 1-benzyl-2-propyldisulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

dibenzyl disulphide (150-60-7) + Dipropyl disulfide (629-19-6) → 1-benzyl-2-propyldisulfane (27657-11-0)

Guidance literature:

With N-fluorobis(benzenesulfon)imide; In 1,2-dichloro-ethane; at 50 ℃; for 4h; Schlenk technique; Sealed tube;

DOI:10.1016/j.cclet.2021.12.073

Reference yield: 62.0%

→ 1-benzyl-2-propyldisulfane (27657-11-0)

Guidance literature:

With N-fluorobis(benzenesulfon)imide; In 1,2-dichloro-ethane; at 50 ℃; for 4h;

Reference yield: 41.0%

benzyl thiocyanate (3012-37-1) + propyl tosylate (599-91-7) → 1-benzyl-2-propyldisulfane (27657-11-0)

Guidance literature:

With potassium phosphate; tetra(n-butyl)ammonium hydroxide; thiourea; potassium iodide; In water; at 90 ℃; for 0.166667h; Microwave irradiation; Green chemistry;

DOI:10.1039/c4ra03592e

upstream raw materials:

1-thiopropane

C₈H₁₀N₂S₂*ClH

dipropyl trisulfide

dibenzyltrisulfide

Refernces

• 1、 Hu, Qingyue,Li, Zheng-Yi,Song, Mengjie,Sun, Xiaoqiang,Yang, Ke. "NFSI-catalyzed S[sbnd]S bond exchange reaction for the synthesis of unsymmetrical disulfides". supporting information. . Retrieved 2022/01/26.
• 2、 Lu, Xiaogang,Wang, Hongmei,Gao, Runli,Sun, Daoming,Bi, Xiaojing. "Microwave-assisted synthesis of asymmetric disulfides". . p. 28794 - 28797. Retrieved 2014/07/22.